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NIR determination of major constituents in tropical root and tuber crop flours

Lebot Vincent, Champagne Antoine, Malapa Roger, Shiley Dan. 2009. Journal of Agricultural and Food Chemistry.
NIR determination of major constituents in tropical root and tuber crop flours
ARTICLE, (2009 ) - PUBLISHEDVERSION - English (en-GB)
Journal of Agricultural and Food Chemistry
OPENACCESS - Cirad license, info:eu-repo/semantics/restrictedAccess, https://agritrop.cirad.fr/mention_legale.html.
Audience : RESEARCHERS
American Chemical Society
Sujet
Q04 - Composition des produits alimentaires, U30 - Méthodes de recherche, F60 - Physiologie et biochimie végétale, Manioc, Taro, Igname, Patate douce, Légume racine, Farine non céréalière, Composition chimique, Teneur en glucides, Teneur en azote, Teneur en éléments minéraux, Amidon, Cellulose, Spectroscopie infrarouge, technique de prévision
Domaines
Agriculture, Biologie, Sciences du vivant, Sciences exactes, Chimie, Agronomie
Description
Tropical root and tuber crops (cassava, sweet potato, taro, and yam) are staples in developing countries where rapid urbanization is strengthening the demand for flour based foods. Quality control techniques are still under development, and when available, laboratory analyses are too expensive. The objectives of this study were to calibrate Near-infrared spectroscopy (NIRS) for routine analysis of flours and to test its reliability to determine their major constituents. Flours prepared from 472 accessions (traditional varieties and breeding lines) were analyzed for their starch, total sugars, cellulose, total nitrogen, and ash (total minerals) contents. The near-infrared (350-2500 nm) spectra of all samples were measured. Calibration equations with cross and independent validation for all analytical characteristics were computed using the partial least squares method. Models were developed separately for each of the four crop species and by combining data from all spp. to predict values within each of them. The quality of prediction was evaluated on a test set of 94 accessions (20%) by standard error of prediction (SEP) and r2 parameters between the measured and the predicted values from cross-validation. Starch, sugar, and total nitrogen content could be predicted, respectively, with 87%, 86%, and 93% confidence, whereas ash (minerals) could be predicted with 71%, and cellulose was not predictable (r2 = 0.31). The statistical parameters obtained for starch, sugars, and total nitrogen are of special interest for flour quality control. These constituents are quantitatively the most important in the chemical composition of flours, and starch content is negatively correlated with sugars and total nitrogen. NIRS is a low cost technique well adapted to the conditions in developing countries and can be used for the high-throughput screening of a great number of samples. Possible applications are discussed. (Résumé d'auteur)
Mots-clés
Cassava, flours, major constituents, NIRS, sweet potato, taro, yam
Langue
English (en-GB)
Auteurs
Lebot Vincent, Champagne Antoine, Malapa Roger, Shiley Dan
Contributeurs
Sources
J. Agric. Food Chem., Vol. 57, No. 22, 2009
Couverture
Vanuatu
Nom du journal
Journal of Agricultural and Food Chemistry